World Journal of
Pharmaceutical and Life Sciences

( An ISO 9001:2015 Certified International Journal )

An International Peer Reviewed Journal for Pharmaceutical and Life Sciences
An Official Publication of Society for Advance Healthcare Research (Reg. No. : 01/01/01/31674/16)
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Abstract

EVALUATION AND VALIDATION OF A UPLC METHOD FOR THE STABILITY INDICATING ASSAY OF MIDOSTAURIN IN IN CAPSULE DOSAGE FORM USING UPLC-MS/MSn

Dr. Osman Ahmed* Khadeeja and Dr. Anas Rasheed

ABSTRACT

This proposal provides a comprehensive review of the optimization and approval of the LCMS technology for
evaluating midostaurin, a chemical that potentially be a tyrosine kinase inhibitor. Analysts had to choose a
permanent and movable stage, as well as develop standard stock and diluent arrangements, in order to find the best
circumstances for division. The study indicated that a BDS C18 provided the best determination and affectability
when combined with slope programming, using a portable stage of methanol and acetonitrile (80:20 v/v). By
analyzing the method's precision, linearity, adaptability, and exactness, the panel also looked at the method's
validity. Considerations of accuracy showed respectable recoveries, with a brutality level of 99.28%. There were
factually irrelevant ponders of correctness that proved the system and approach were accurate.

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